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The report on the performed work



To give the scheme of technological process (with the indication of the modes) productions of this type of a product. To describe performance of work on a task, to give necessary calculations and to fill in the technological magazine and the magazine of quality control. To carry out the analysis of the received results and to explain them.To make the short conclusion on work.

Control questions:

1. Ways of production of fermented milk products.

2. Technological modes of production of fermented milk products. Their justification and influence on quality of a ready-made product.

3. What types fermentation are the cornerstone of production of fermented milk products?

4. The mechanism of formation of a clot when souring milk.

5. Defects of fermented milk products. Reasons of their emergence

Laboratory work № 10

The study of the technologies of sour cream

The purpose was practically to get acquainted with technological process of production of sour cream, methods of quality control, to study the effect of homogenization of cream and their advanced physical maturation on the consistency of the product.

Task 1. To investigate the influence of mode of homogenization to the consistency of sour cream.

Task 2. To study the effect of prior physical ripening of cream to the consistency of sour cream.

 

Short theoretical data

Sour cream is produced from normalized pasteurized cream by fermentation with starter prepared on pure cultures of lactic acid bacteria and ripening at low temperatures. Depending on the microflora of the leaven and the mass fraction of fat sour cream produce the following types:

 

Table 10.1

 

Mass fraction of fat Sourdough microflora (lactic acid cocci) The temperature of fermentation, °C Acidity, °Т
Mesophilic and thermophilic 28–32 70-100
Mesophilic and thermophilic 28–32 65-100
Mesophilic 22–28 65-100
Mesophilic 22-28 60-100
Mesophilic 22-28 60-100
Mesophilic and thermophilic 39-41 65-85

 

Sour cream with fat mass fraction of 10, 15 and 20 % can be produced from a mixture of cow's cream and soy protein. The mixture ferment cultures of mesophilic lactic acid streptococci. Soy protein is added to cream to improve the texture of the finished product. For cream with fat mass fraction of 10, 15 and 20 % mass fraction of soy protein is respectively to 5-6, 3-4 and 2-3 kg per 1000 kg of finished product. Sour cream with soy protein produced the same way as sour cream from cow's cream. Shelf life of sour cream in sealed container up to 7 days.

On organoleptic and physico-chemical properties cream must conform to the requirements specified in table.10.2 and 10.3.

Organoleptic indicators of sour cream Table10.2

Name of indicator Characteristic
Taste and smell Clean sour milk without any foreign tastes and odors. For products from recombined cream is allowed to taste ghee
Color White with cream tint, uniform throughout the mass
The consistency and appearance Homogeneous dense mass with glossy surface

 

Physical and chemical properties of sour cream Table10.3

Name of indicator The norm for a product with a mass fraction of fat, %
10–14 15–19 20–34 35–48 50–58
Mass fraction protein, %, not less 3, 0 2, 8 2, 6 2, 4 2, 2
Acidity, º Т From 60 to 90 From 60 to 100
The temperature on leaving the enterprise, º С   4±2
Phosphatase Absent

 

Among other sour milk products sour cream has high nutritional qualities. Due to the changes of the protein during the fermentation process, cream is absorbed by the body faster and easier than a cream appropriate cream. Sour cream is produced the reservoir, and thermostatic means. Tank (more economical and allows to obtain a more uniform quality of product by units of packaging compared to incubation) the method of production of sour cream consists of following technological operations: receiving and preparation of raw materials; separation of milk, obtaining and normalizing cream; pasteurization, homogenization and cooling cream, fermentation and ripening of cream; mixing fermented cream, packaging and labeling, cooling and maturation of sour cream.

 

Equipment, devices and technical facilities:

Cream with fat content of 20-25 %; cow milk; starter culture for sour cream, reagents and apparatus for determination of titratable acidity and the mass fraction of fat in milk and cream, centrifuge tubes, consistometer, thermometers, thermostats, valve homogenizer; measuring cups, cylinders, buckets, whorls, glass beakers with a capacity of 250 ml.

The work order

Syneresis properties – 10 ml of the investigated product is placed in a measuring tube and centrifuged for 30 min, determining every 5 min the volume of the evolved serum, constructing a graph characterizing the intensity of syneresis;

The consistency of sour cream assess consistometer method of spreading. To do this, in the centre of the consistometer install hollow metal cylinder, fill it with product. Then the cylinder is lifted above the surface of the consistometer, and after two minutes measure the diameter of the spreading of sour cream.

The efficiency of homogenization is determined by centrifugation in a special pipette. The pipette through the lower capillary end is filled with the sample of cream to the top mark. The upper end of the pipette is closed with the finger, and the lower end put on the rubber stopper. Filled pipette is inserted symmetrically in the cartridges are centrifuge tubes to the periphery. After centrifugation, the pipette is removed and put vertically on the tube in the lower end. Then pipette carefully, without turning and shaking, drained the lower part of the product to the lower level, which closed with a finger of the left hand the upper opening of the pipette, and the right to remove the rubber plug from the lower end of the pipette. The merged product will determine the fat content. Homogeneity is calculated by the formula:

 

Эг = 100 Жнпр,

 

where, Эг is the degree of homogenization, %; Жн – mass fraction of fat in the lower layer of the product discharged from the pipette %; Жпр – fat content in product, %.

Study of the effect of mode of homogenization to the consistency of sour cream. Pasteurized cream is cooled to a temperature of 70 º C and homogenize, divide into 3-4 pieces and homogenizer at a pressure of 5, 10, 15 MPa. One part cream not homogenizers. Take samples of cream and determine the efficiency of homogenization. Of homogenised at different pressures and negalogenizirovanny cream produced under the same conditions cream.

After homogenization the cream immediately cooled to the fermentation temperature of 25-27 ° C and make the leaven of pure cultures for sour cream in an amount of 5 %. The mixture was stirred and left to ripen in the thermostat to clot formation. The stirring was repeated after 1 h after fermentation.

Upon reaching the titratable acidity 60-65 º Т fermented cream is stirred and cooled to 5-6 ° C and kept for ripening. In the finished sour cream determine the mass fraction of fat, acidity, sinergeticheskie properties, the diameter of the spreading. Assess sensory characteristics.

Study of the effect of prior physical ripening of cream to the consistency of sour cream. Pasteurized cream was cooled to 25-26 ° C and divided into two equal parts. One of them make a bacterial ferment in the amount of 5 %, mix and leave to ripen in the thermostat to clot formation.

The second portion of cream is cooled to low temperature tap water and placed in the freezer refrigerator. After an hour take out the cream from the refrigerator, measure their temperature, slowly heated to a temperature of 25-26 ° C, make the leaven in the amount of 5 %, mix and leave to ripen in the thermostat to clot formation.

In both samples, the mixing was repeated after 1 h after fermentation. Upon reaching the titratable acidity 60-65 º Т sour cream stand in the refrigerator. After cooling to 6 ° C carried out the quality assessment of sour cream determine the mass fraction of fat, acidity, diameter spreading. Assess sensory characteristics.

Determination acidity of sour cream.

1. On technical scales weigh in a beaker 5 g of sour cream, add 40 ml of water, 3 drops of phenolphthalein, mix well with a glass rod.

2. The mixture in a glass of titrate burettes 0.1N. NaOH solution until not disappear within 1 minute weak-pink color.

3. Read off the amount of alkali (ml) that went to the titration. Multiply the result by 20, we get acidity in Turner degrees. The discrepancy between two parallel determinations should be no more than 2 ° T.

 

The report on the done work

 

Make the scheme of the technological process of production of sour cream. Perform the necessary calculations. The results of observations and analyses recorded in the form presented in table 10.4. Build a graph characterizing the intensity of syneresis. Make a conclusion about the effect of homogenization on the consistency of sour cream.

Table 10.4

Number of the sample The mode of homogenization The efficiency of homogenization, % Indicators of sour cream
Temperature, ° С Pressure, МПа Acidity, º Т Consistency in diameter spread mm Taste and aroma Appearance
             
             
             
             

Laboratory work № 10


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